RT Journal Article
T1 Small-angle neutron scattering study of the nano-sized features in an oxide dispersion-strengthened Fe12Cr alloy
A1 Pareja Pareja, Ramiro
A1 Parente, Paola
A1 Muñoz Castellanos, Ángel
A1 Radulescu, A
A1 Castro Bernal, María Vanessa de
AB Small-angle neutron scattering experiments, along with positron lifetime measurements and transmission electron microscopy observations, were performed on samples of an oxide dispersion-strengthened (ODS) Fe12Cr alloy and its non-ODS counterpart in order to characterize their nano-sized features. The nuclear and magnetic scattering data were analysed using the maximum entropy approach for obtaining the size distribution of the scattering centres in these materials. The positron annihilation results and the TEM information have made possible an interpretation of the volume distribution of the scattering centres having sizes below ~16nm and their proper quantitative analyses. The smaller scattering centres in the ODS alloy exhibit distributions with modal values at ~6-7 and 12-14nm. The peak at ~6-7nm appears to be due to the overlapping of more than one type of scattering centres, while the one at ~12-14nm can be exclusively attributed to the Y-rich centres. The quantitative analysis of the magnetic scattering data yields a volume fraction and number density of the Y-rich particles estimated in 0.70 +/- 0.03% and 0.77x10(22)m(-3), respectively.
PB Taylor & Francis Online
SN 1478-6435
YR 2015
FD 2015-08-03
LK https://hdl.handle.net/10016/31988
UL https://hdl.handle.net/10016/31988
LA eng
NO This investigation was supported by the Spanish Ministry of Science and Innovation [grant number ENE2010-17462]; Comunidad de Madrid through the program ESTRUMAT-CM [grant number S2009/MAT-1585]; European Union under the 7th Framework Program [grant number 312483]; and ESTEEM2 (Integrated Infrastructure Initiative-I3) and the Royal Society International Exchanges Scheme 2011/R1 [grant number IE110136].
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RD 27 jul. 2024