Citation:
Šćepanović, M., Leguey, T., Auger, M. A., Lozano-Perez, S., Armstrong, D.E.J., García-Cortés, I. y Castro, V. de. (2018). Characterisation of ODS Fe-14Cr-2W-0.3Ti before and after high temperature triple and low temperature single ion irradiations. Materials Characterization, 136, pp. 318-330.
xmlui.dri2xhtml.METS-1.0.item-contributor-funder:
Comunidad de Madrid Engineering and Physical Sciences Research Council (EPSRC) European Commission Ministerio de Economía y Competitividad (España)
Sponsor:
This investigation was supported by the Ministerio de Economía y Competitividad (project ENE2015-70300-C3-2-R), the Comunidad de Madrid through the program TECHNOFUSION-II (S2013/MAE-2745), the UK Engineering and Physical Sciences Research Council (EPSRC) (Refs: EP/H018921/1 and EP/M022803/1) and the European Union Seventh Framework Programme under Grant Agreement 312483 - ESTEEM2 (Integrated Infrastructure Initiative – I3).
The authors acknowledge the JANNuS-Saclay and the CMAM team for their and technological advice. DEJA acknowledges support through a Royal Academy of Engineering Research Fellowship. MA acknowledges Dr A.J. London for providing MatLab codes.
Project:
Comunidad de Madrid. S2013/MAE-2745 Gobierno de España. ENE2015-70300-C3-2-R info:eu-repo/grantAgreement/EC/FP7/312483
Keywords:
Oxide dispersion strengthened steels
,
Ion irradiation
,
Transmission electron microscopy
,
Nanoindentation
,
Atom probe tomography
,
Nanoparticles
Oxide dispersion strengthened reduced activation ferritic steels are being considered as structural materials for future fusion reactors and Gen IV fission reactors. In this work, the stability of the nanometric oxides after being irradiated at different condiOxide dispersion strengthened reduced activation ferritic steels are being considered as structural materials for future fusion reactors and Gen IV fission reactors. In this work, the stability of the nanometric oxides after being irradiated at different conditions and temperatures has been investigated. A Fe-14Cr-2W-0.3Ti-0.3Y(2)O(3) alloy was simultaneously triple-beam irradiated at 600 degrees C with Fe, He and H ions. The same alloy was irradiated with Fe ions at -80 degrees C. The microstructure of this alloy was investigated using Transmission Electron Microscopy, Atom Probe Tomography and nanoindentation before and after the irradiations. There were no significant changes in the morphology and chemical composition of the nanoparticles after the irradiations, although the size of the smaller ones tends to decrease for both irradiation conditions. Small irradiation-induced bubbles were present after the triple simultaneous irradiation at high temperature. Nanoindentation also shows no significant differences with a slight increase in hardness for the sample irradiated at low temperature, while softening appears in the high temperature irradiation.[+][-]