Publication: Phase diagrams in alternative hard materials: Validation of thermodynamic simulation through high temperature x-ray diffraction, differential thermal analysis and microstructural characterization
dc.affiliation.dpto | UC3M. Departamento de Ciencia e Ingeniería de Materiales e Ingeniería Química | es |
dc.affiliation.grupoinv | UC3M. Grupo de Investigación: Tecnología de Polvos | es |
dc.contributor.author | Nicolás Morillas, María de | |
dc.contributor.author | Pereira, L. | |
dc.contributor.author | Penoy, M. | |
dc.contributor.author | Bertalan, C. | |
dc.contributor.author | Useldinger, R. | |
dc.contributor.author | Llanes, L. | |
dc.contributor.author | Gordo Odériz, Elena | |
dc.contributor.funder | Ministerio de Economía y Competitividad (España) | es |
dc.contributor.funder | Comunidad de Madrid | es |
dc.contributor.funder | Ministerio de Ciencia e Innovación (España) | es |
dc.date.accessioned | 2021-05-04T10:45:46Z | |
dc.date.available | 2023-06-01T23:00:06Z | |
dc.date.issued | 2021-06 | |
dc.description.abstract | In this investigation, Ti(C,N)-FeNiCr systems were designed using Thermo-Calc® software. Materials were processed by conventional powder metallurgy, employing different carbon additions to study a wide range of the phase diagram as well as the effect of C in the sintered samples. Specimens were extensively characterised in terms of density, magnetic and mechanical properties, and microstructural features. Simulation approach was validated by means of Differential Thermal Analysis (DTA) and High-Temperature X-Ray Diffraction (HT-XRD), from room temperature up to 1200 °C for each composition, comparing phases obtained for each temperature and composition with predicted ones. Results showed excellent consonance between Thermo-Calc® and XRD phases, except for precipitation of secondary carbides, which appeared in the simulation but not in the sintered samples. Moreover, variation of C content demonstrated to have a direct effect in the microstructural homogenization of the final specimens. | en |
dc.description.sponsorship | The current study was supported by the Spanish Government through the projects MAT2015-70780-C4-P and PID2019-106631GB-C41/C43, and grant BES-2016-077340, and the Regional Government of Madrid through the program ADITIMAT, ref. S2018/NMT-4411. The authors would like to thank BASF for providing the iron powder used in this investigation. | en |
dc.format.extent | 10 | |
dc.identifier.bibliographicCitation | de Nicolás, M., Pereira, L., Penoy, M., Bertalan, C., Useldinger, R., Llanes, L. & Gordo, E. (2021). Phase diagrams in alternative hard materials: Validation of thermodynamic simulation through high temperature x-ray diffraction, differential thermal analysis and microstructural characterization. International Journal of Refractory Metals and Hard Materials, 97, 105513. | en |
dc.identifier.doi | https://doi.org/10.1016/j.ijrmhm.2021.105513 | |
dc.identifier.issn | 0263-4368 | |
dc.identifier.publicationfirstpage | 1 | |
dc.identifier.publicationissue | 105513 | |
dc.identifier.publicationlastpage | 10 | |
dc.identifier.publicationtitle | International Journal of Refractory Metals and Hard Materials | en |
dc.identifier.publicationvolume | 97 | |
dc.identifier.uri | https://hdl.handle.net/10016/32526 | |
dc.identifier.uxxi | AR/0000027285 | |
dc.language.iso | eng | |
dc.publisher | Elsevier | en |
dc.relation.projectID | Gobierno de España. BES-2016-077340 | es |
dc.relation.projectID | Comunidad de Madrid. S2018/NMT-4411 | es |
dc.relation.projectID | Gobierno de España. MAT2015-70780-C4-P | es |
dc.relation.projectID | Gobierno de España. PID2019-106631GB-C41 | es |
dc.relation.projectID | Gobierno de España. PID2019-106631GB-C43 | es |
dc.rights | © 2021 Elsevier Ltd. | en |
dc.rights | Atribución-NoComercial-SinDerivadas 3.0 España | * |
dc.rights.accessRights | open access | |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/3.0/es/ | * |
dc.subject.eciencia | Materiales | es |
dc.subject.eciencia | Química | es |
dc.subject.other | Cermets | en |
dc.subject.other | Ti(C,N) | en |
dc.subject.other | Alternative binders | en |
dc.subject.other | Phase diagram simulation | en |
dc.subject.other | High-temperature XRD | en |
dc.title | Phase diagrams in alternative hard materials: Validation of thermodynamic simulation through high temperature x-ray diffraction, differential thermal analysis and microstructural characterization | en |
dc.type | research article | * |
dc.type.hasVersion | AM | * |
dspace.entity.type | Publication |
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